An irresolute linker: separation, and structural and spectroscopic characterization of the two linkage isomers of a Ru(ii)-(2-(2′-pyridyl)pyrimidine-4-carboxylic acid) complex

For the fi rst time the two linkage isomers of a Ru( II ) complex with 2-(2 ’ -pyridyl)pyrimidine-4-carboxylic acid (cppH) – that form in comparable amounts – have been fully characterized individually. The X-ray structure of each isomer is related to its NMR spectrum in solution.



Titolo: An irresolute linker: separation, and structural and spectroscopic characterization of the two linkage isomers of a Ru(ii)-(2-(2′-pyridyl)pyrimidine-4-carboxylic acid) complex
Autori: 
IENGO, ELISABETTA
BALDUCCI, GABRIELE
ALESSIO, ENZO
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Data di pubblicazione: 2014
Rivista: 
DALTON TRANSACTIONS  
Abstract: For the fi rst time the two linkage isomers of a Ru( II ) complex with 2-(2 ’ -pyridyl)pyrimidine-4-carboxylic acid (cppH) – that form in comparable amounts – have been fully characterized individually. The X-ray structure of each isomer is related to its NMR spectrum in solution.
Handle: http://hdl.handle.net/11368/2798729
Digital Object Identifier (DOI): http://dx.doi.org/10.1039/c4dt01282h
URL: http://pubs.rsc.org/en/journals/journalissues/dt#!issueid=dt044048&type=current&issnprint=1477-9226
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